Humboldt-Universität zu Berlin - Faculty of Mathematics and Natural Sciences - NMR Spectroscopy

AVANCE DPX 300MHz

 

 

 

After an introductory instruction by the NMR service personnel all employees, phd students, Bachelor and Master students are allowed to measure at the 300 MHz DPX spectrometer on their own. Please get in contact with Jana Hildebrandt for an introduction.

 

The DPX is accessible 24/7. Please book time slots for measurements here with your HU Account details.
Measurements at the DPX should not exceed 30min. For longer measurements the Autosampler should be used or a time slot after 5pm be booked.

 

For all samples the instructions for sample preparation have to followed.

 

At the DPX spectrometer the following experiments are possible:

 

1D: 1H, 13C, DEPT, APT, 19F, 31P

2D homonuclear: H,H-COSY

High temperature measurements up to +100°C

Low temperature measurements up to -80°C

 

For the low temperature measurements a separate instruction course by the NMR service personnel is mandatory. Please get in contact with Dr. Dallmann.