AVANCE DPX 300MHz
After an introductory instruction by the NMR service personnel all employees, phd students, Bachelor and Master students are allowed to measure at the 300 MHz DPX spectrometer on their own. Please get in contact with Jana Hildebrandt for an introduction.
The DPX is accessible 24/7 apart from thursdays between 7:30 and 9am.
Measurements at the DPX should not exceed 20min. Longer measurements will be measured automatically at night, i.e. after 6pm.
For all samples the instructions for sample preparation have to followed.
At the DPX spectrometer the following experiments are possible:
1D: 1H, 13C, DEPT, APT, 19F, 31P, 11B
2D homonuclear: H,H-COSY, H,H-TOCSY, H,H-NOESY
2D heteronuclear: H,C-HSQC, H,C-HMBC
High temperature measurements up to +100°C
Low temperature measurements down to -80°C
For the low and high temperature measurements a separate instruction course by the NMR service personnel is mandatory. Please get in contact with Dr. Dallmann.
The current load of the 300 NEO can be checked here online with login Service/xw1n.2d in order to avoid unnecessary travel to the magnet.
For 19F und 31P-measurements you can find a table with respective reference values.